Description
The FCC Micro Activity Test (MAT) system is designed to assess the performance of FCC catalysts by evaluating their activity and selectivity during catalytic cracking reactions. It measures how efficiently heavy hydrocarbons, such as vacuum gas oil (VGO), are converted into lighter products including gasoline, LPG, cycle oils, and coke, while providing detailed information on product distribution. The device includes a separate injection line equipped with a dedicated syringe pump for biomass, allowing precise co-processing of bio-oils with conventional FCC feeds.. The system also enables researchers to investigate how operating parameters—such as temperature, pressure, feed composition, and flow rates—influence catalyst behavior. By allowing the testing and comparison of various commercial or laboratory-developed catalysts and feedstocks, the MAT unit supports catalyst development, refinery process optimization, and research activities. The system is designed in compliance with ASTM D3907 and ASTM D5154 standards. In operation, a small amount of catalyst (approximately 4 g) is first loaded into a quartz fixed-bed reactor. The reactor is then heated to the desired cracking temperature, typically around 516 °C, while nitrogen is used to purge the system and remove air. Once stable operating conditions are reached, a hydrocarbon feed such as vacuum gas oil is injected into the heated reactor using a controlled injection system. Upon contact with the catalyst, catalytic cracking reactions occur, breaking large hydrocarbon molecules into smaller compounds. This reaction produces gaseous products, liquid hydrocarbons, and coke deposited on the catalyst. The reactor effluent then enters a separation section, where liquid products are condensed and collected, while the gas phase is accumulated and analyzed, typically using a micro gas chromatograph. After the reaction, the coke deposited on the catalyst is burned off using air, which regenerates the catalyst and allows the coke yield to be measured. Finally, the system compiles the analytical data to generate a comprehensive report, including conversion rates, product yields, and catalyst performance indicators.
Features
Reactor
Reactor type: Quartz fixed-bed
Catalyst capacity: up to 10 mL
Typical catalyst load: ~4 g (≈7 mL)
Catalyst/Oil ratio: 1–6 g/g
Pressure: Near atmospheric
Furnace with three independent heaters:
Typical operating temperature: ~516 °C
Maximum capability: up to ~800 °C
Temperature accuracy: ±1 °C
Automated Feed Injection
Injection duration: 20 seconds to more than 1 minute
Feed control: Coriolis mass flow controller for precise feed measurement
Heated feed lines: Up to 100 °C to handle heavy feedstocks such as Vacuum Gas Oil (VGO)
Advanced Product Collection System
Gas and liquid products automatically separated
Liquid receivers placed in ice-cooled bath
Gas collected in a stainless-steel accumulator (Mariotte vessel) for volume measurement
Integrated air line for catalyst regeneration:
Air flow: 0.6 – 6 Nl/h
CO₂ measurement: via a infrared gas analyzer
Integrated Analytical Capabilities
Optional Micro Gas Chromatograph (µGC) for real-time gas composition analysis
N₂
CH₄
C₂–C₄ hydrocarbons
C₅–C₆ hydrocarbons
Liquid product analysis using SIMDIST (ASTM D2887) to determine:
Gasoline fraction (< 216 °C)
Light Cycle Oil (216–343 °C)
Heavy Cycle Oil (> 343 °C)
Catalyst Regeneration and Coke Measurement
In-situ catalyst regeneration via air burn-off
Infrared analyzer measures CO₂ to determine coke yield
Automated Multi-Run Operation
Supports 4–8 automatic test runs
Fully automated operation with detailed reporting
Benefits
* Accurate Catalyst Evaluation: Provides reliable measurements of catalyst activity, selectivity, and coke formation.
* Industrially Relevant Data: Replicates key FCC reaction conditions to produce data representative of refinery performance.
* Reduced Catalyst Consumption: Requires only a few grams of catalyst, enabling cost-effective testing.
* High Repeatability: Precise temperature control, automated feed injection, and advanced flow control ensure consistent and reproducible experiments.
* Flexible Feedstock Testing: Compatible with:
Vacuum gas oil (VGO)
Atmospheric gas oil (AGO)
Residue mixtures
Bio-oil co-processing (optional configuration).
* Comprehensive Product Analysis : Delivers a complete material balance including gas, liquid, and coke yields, allowing detailed process and catalyst optimization.
* Automated Operation: Multi-run capability and integrated software allow unattended testing and automated reporting.