SH-Slurry hydrocracking pilot plant for bio-based and fossil feedstock

Description

Vinci Technologies offers a continuous slurry hydrocracking pilot plant for heavy residue hydroconversion.  The system is designed to process vacuum residue, extra-heavy oils and other challenging feedstocks such as biomass-derived oils (e.g., pyrolysis oil). It supports catalyst development, process optimization and comparative hydroconversion studies.  A 2 L stirred reactor provides controlled contact between heavy oil, dispersed catalyst and hydrogen.  The reactor operates at pressures from 30 to 200 bar, with heating capability up to 500 °C.  Mechanical agitation maintains catalyst suspension and promotes gas–liquid contact.  Feedstock throughput reaches 5 L/h, with independent catalyst slurry injection up to 600 mL/h.  Hydrogen flow is controlled between 500 and 5,000 NL/h to suit the experimental conditions.  A dedicated compressor supplies hydrogen at pressures up to 220 bar.  Two agitated preparation vessels accommodate oil-soluble catalyst precursors and powder suspensions.  Heated, nitrogen-blanketed feed and slurry tanks maintain suitable conditions for viscous materials.  A heated syringe pump provides precise delivery of the catalyst suspension to the reactor.  An optional operating configuration uses the removable Robinson–Mahoney basket to test extrudate catalysts.  The unit also supports catalyst-free operation for comparative thermal cracking studies.  A high-pressure, high-temperature separator recovers the heavy fraction containing dispersed catalyst.  Following pressure let-down, a cooled separator recovers condensed hydrocarbons and water separately.  Weighed collection vessels and dry gas metering provide measurements for experimental mass balances.  PLC control and PC supervision provide operating trends, data logging and alarm management.  Multiple safety layers include independent temperature protection, emergency shutdown and pressure relief devices.  

Features

Applications: slurry hydrocracking and hydroconversion of vacuum residue, extra-heavy oils and heavy feedstocks.
Operating modes: slurry, catalyst-free thermal cracking and Robinson–Mahoney catalyst basket.
Reactor capacity: 2 L.
Operating pressure: 30–200 bar; design pressure: 220 bar.
Heating capability: up to 500 °C, including reactor flange and bottom.
Agitation speed: up to 1,000 rpm.
Feedstock flow rate: up to 5 L/h.
Slurry injection: independent heated syringe pump, up to 600 mL/h.
Hydrogen flow rate: 500–5,000 NL/h.
Hydrogen compressor: up to 220 bar discharge pressure.
Catalyst preparation: two agitated vessels of 5 L and 20 L.
Feed and slurry tanks: 250 L each, heated, nitrogen-blanketed and fitted with weighing scales.
Hot separator: 1.5 L, operating at 30–200 bar and 350–480 °C.
Cold separator: 1.5 L, operating at 0–5 bar, with chilled head.
Product recovery: separate collection of heavy hydrocarbons, light hydrocarbons and water.
Sampling and analysis: automatic liquid sampling, dry gas metering and external GC connection.
Automation: PLC and PC supervision with data logging, trends, alarms and mass-balance functions.
Safety: emergency shutdown, hydrogen isolation, nitrogen purge, temperature protection and pressure relief devices.
Construction: primarily 316/316L stainless steel, with polycarbonate enclosure.
Continuous operation: designed for runs of 100 hours or more.
Approximate dimensions: 5 m × 2 m × 3 m.

Benefits

* Evaluate challenging feedstocks: investigate the hydroconversion of vacuum residues and extra-heavy oils using dispersed catalysts.
* Compare catalyst technologies: assess slurry catalysts, extrudates in Robinson–Mahoney mode and catalyst-free thermal cracking on the same platform.
* Optimize process conditions: independently adjust temperature, pressure, hydrogen flow and catalyst dosage to study their effects on conversion and product quality.
* Collect reliable experimental data: combine separate product recovery, weighing, gas metering and continuous logging to establish mass balances.
* Support extended testing: automated control, heated feed handling and multiple safety layers enable continuous campaigns of 100 hours or more.