Description
This pilot plant is a skid-mounted, modular unit designed for the flexible and safe production of low- to mid-molecular-weight polyesters at pilot scale. With a typical capacity of approximately 50 kg per batch, the unit provides an industrially representative platform for process development, optimization, and scale-up. Fully assembled and tested prior to delivery, the skid-mounted design minimizes on-site installation time and ensures rapid project deployment. The process is based on a multi step batch operation. In the first step, a base ester is produced in a loop reactor through controlled esterification of acids and glycols. Efficient heat transfer and mixing are ensured by a circulating loop equipped with pumps, heat exchangers, and a separator vessel. Reaction water is continuously removed using an integrated distillation column, driving the reaction to completion and enabling alcohol recovery and recycle for improved efficiency
In further steps, the base ester is converted into polyester by gradually reducing pressure and adjusting operating conditions to initiate polymerization. The process allows precise control of molecular weight, supported by online analytical tools that define the reaction endpoint. Multiple hot oil circuits provide accurate temperature control across the reactor, piping, and distillation systems, ensuring stable and reproducible operation.
Features
Batch pilot unit for low- to mid-molecular-weight polyester development (~50 kg per batch)
Pressurized loop reactor operating up to ~100 psig during esterification for efficient heat and mass transfer
Multi stage operation with controlled transition from esterification to polymerization via gradual pressure reduction
Precise temperature control using multiple hot-oil circuits for reactor, piping, column, and reboiler
Integrated distillation column for continuous removal of reaction water and alcohol recycle
Flexible operating window supporting multiple acids, glycols, solvents, and bio-based feedstocks
Real-time reaction monitoring compatibility (viscosity, NIR) for accurate molecular-weight control
Industrial-grade design with 316L stainless steel construction, Class 1 Division 2 compliance, and full
Benefits
Industrial-scale relevance: ~50 kg/batch capacity with multi-step batch processing, ideal for polyester process development and scale-up.
High process control & product quality: Precise temperature, pressure, and molecular-weight control with online analytics ensures reproducible polyester properties.
Fast and efficient deployment: Skid-mounted, fully tested unit with integrated distillation and recycle minimizes installation time and improves process efficiency.